3,3′-Sulfonyldianiline (CAS 599-61-1): Comprehensive User Guide
Table of Contents
1. Product Overview & Specifications
Chemical Name: 3,3′-Sulfonyldianiline
CAS Number: 599-61-1
Molecular Formula: C12H12N2O2S
Molecular Weight: 264.3 g/mol
Appearance: White to pale yellow crystalline powder
Melting Point: 120-124°C
Solubility: Soluble in DMF, DMSO; slightly soluble in water
Comparative Analysis
| Parameter | 3,3′-Sulfonyldianiline | 4,4′-Sulfonyldianiline | m-Phenylenediamine |
|---|---|---|---|
| Thermal Stability | Excellent (>300°C) | Good (>280°C) | Moderate (>250°C) |
| Solubility in DMF | High | Moderate | Low |
| Reactivity | Controlled | Fast | Variable |
2. Key Applications & Use Cases
Core Applications:
- Polymer Intermediate: Critical for high-performance polyimides and epoxy resins
- Thermoset Curing Agent: Enables precise crosslinking in aerospace composites
- Pharmaceutical Synthesis: Key intermediate for antitumor agents and kinase inhibitors
- Liquid Crystal Polymers: Enhances thermal stability in display technologies
3. Step-by-Step Usage Examples
Example 1: Epoxy Resin Formulation
- Mix 3,3′-Sulfonyldianiline (10-15% w/w) with DGEBA epoxy resin
- Stir at 80°C for 30 minutes under nitrogen atmosphere
- Cure at 150°C for 2 hours followed by 180°C post-cure
Example 2: Polyimide Synthesis
- React with pyromellitic dianhydride in NMP solvent
- Maintain stoichiometric ratio (1:1) at 50°C for 6 hours
- Imidize at 300°C under vacuum to achieve 95% conversion
4. Real-World Customer Case Studies
Case Study 1: Aerospace Composite Manufacturer
Client: Top 3 global aerospace materials supplier
Challenge: Required curing agent with 320°C+ stability
Solution: Custom 3,3′-Sulfonyldianiline formulation
Result: 22% weight reduction in engine components
Case Study 2: OLED Display Producer
Client: Leading Korean electronics firm
Challenge: Needed LC polymer with <0.5% thermal degradation
Solution: Optimized purification protocol (99.8% purity)
Result: Extended display lifespan by 40%
5. Request Technical Specifications
Contact our chemical engineering team for:
– Batch-specific COA
– Custom synthesis options
– Regulatory support documentation
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